Articles written in Journal of Chemical Sciences
Volume 127 Issue 12 December 2015 pp 2269-2282
Synthesis of 𝑁-acylurea derivatives from carboxylic acids and 𝑁,𝑁' -dialkyl carbodiimides in water
Ali Ramazani Fatemeh Zeinali Nasrabadi Aram Rezaei Morteza Rouhani Hamideh Ahankar Pegah Azimzadeh Asiabi Sang Woo Joo Katarzyna Ślepokura Tadeusz Lis
Reactions of benzoic acid derivatives and (𝐸)-cinnamic acid derivatives with 𝑁, 𝑁'-dialkyl carbodiimide proceed smoothly at room temperature and in neutral conditions to afford 𝑁-acylurea derivatives in high yields. The reaction proceeds smoothly and cleanly under mild conditions and no side reactions were observed.
Volume 130 Issue 12 December 2018 Article ID 0166
Tetramethylguanidine-functionalized silica-coated iron oxide magnetic nanoparticles catalyzed one-pot three-component synthesis of furanone derivatives
HAMIDEH AHANKAR ALI RAMAZANI NADIA FATTAHI KATARZYNA SLEPOKURA TADEUSZ LIS PEGAH AZIMZADEH ASIABI VASYL KINZHYBALO YOUNES HANIFEHPOUR SANG WOO JOO
Tetramethylguanidine-functionalized silica-coated iron oxide magnetic nanoparticles as aproductive and reusable catalyst have been applied for the one-pot three-component synthesis of furanone derivatives (4a–o). In addition to the characterization of all products by FT-IR,1HNMR and 13CNMR spectroscopy, single-crystal X-ray analysis of ethyl 5-oxo-2-phenyl--(phenylamino)-2,5-dihydrofuran-3-carboxylate product has been made. Easy recrystallization and good-to-excellent yields (81–92%) of furanone derivatives are notable characteristics of this procedure. The catalyst identification was performed using FT-IR,XRD, SEM, TEM and TGA techniques. It is worth noting that the nanocatalyst can be recycled with an external magnet and reused for several times.
Volume 135, 2023
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