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Volume 25 Issue 3 June 2002 pp 213-217 Alloys and Steels
XRD and TEM analysis of microstructure in the welding zone of 9Cr–1Mo–V–Nb heat-resisting steel
Li Yajiang Wang Juan Zhou Bing Feng Tao
Under the condition of tungsten inert gas shielded welding (TIG) + shielded metal arc welding (SMAW) technology, the microstructure in the welding zone of 9Cr–1Mo–V–Nb (P91) heat-resisting steel is studied by means of X-ray diffractometry (XRD) and transmission electron microscopy (TEM). The test results indicate that when the weld heat input (𝐸) of TIG is 8.5 ∼ 11.7 kJ/cm and the weld heat input of SMAW is 13.3 ∼ 21.0 kJ/cm, the microstructure in the weld metal is composed of austenite and a little amount of 𝛿 ferrite. The substructure of austenite is crypto–crystal martensite, which included angle. There are some spot precipitates in the martensite base. TEM analysis indicates that the fine structure in the heat-affected zone is lath martensite. There are some carbides (lattice constant, 1.064 nm) at the boundary of grain as well as inside the grain, most of which are Cr23C6 and a little amount of (Fe, Me)23C6.
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Bulletin of Materials Science
Volume 46, 2023
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Posted on October 12, 2020Prof. Subi Jacob George — Jawaharlal Nehru Centre for Advanced Scientific Research, Jakkur, Bengaluru
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