Articles written in Bulletin of Materials Science

    • Controlling of morphology of Ni/Al-LDHs using microemulsionmediated hydrothermal synthesis

      Yun Zhao Fenfei Xiao Qingze Jiao

      More Details Abstract Fulltext PDF

      A quaternary microemulsion, cetyltrimethylammonium bromide (CTAB)/water/𝑛-hexane/𝑛-hexanol, was selected for the synthesis of Ni/Al-layered double hydroxides (LDHs). Ni/Al-LDHs with nanowire-, spherical-, rod- and tube-like morphologies were prepared via the microemulsion-mediated hydrothermal synthesis. The CTAB concentration played an important role in determining the morphology of Ni/Al-LDHs. The structure, composition and morphology of the obtained Ni/Al-LDH nanostructures were investigated by X-ray diffraction, inductively coupled plasma emission spectroscopy, infrared spectrometer and transmission electron microscopy. A possible formation mechanism of Ni/Al-LDH nanostructures is proposed.

    • Large-scale synthesis of dual sensing nitrogen-doped graphene quantum dots for real-time detection of pH and antibiotic


      More Details Abstract Fulltext PDF

      Recently, graphene quantum dots (GQDs) with bright fluorescence have emerged as a novel carbon nanomaterial because of their distinctive optical properties and robust chemical inertness. Herein, a simple bottom-upapproach is used to prepare nitrogen-doped GQDs (N-GQDs) by using citric acid as the carbon source and tris (hydroxymethyl) aminomethane (Tris) as the nitrogen source. The prepared N-GQDs have a high yield of 61.50% and the quantum yield is 14.42%. Meanwhile, the N-GQDs exhibit clearly fluorescence quenching with the increase of pH value from 3.0 to 12.0. In addition, the N-GQDs possess excellent fluorescence quenching response to tetracycline (TC) due to the inner filter effect. And the fluorescence intensity of N-GQDs exhibits a good linear relationship with the addition of TC in range of 1–50 ${\mu}$M. The detection limit is determined to be 94 nM. Furthermore, the smartphone-based handheld device is developed to track the fluorescence colour changes caused by the variation of pH and TC. Through analysing the RGB values from the fluorescence images, good linearity betweenRGB values and pH values is obtained ($R^2$ = 0.996), while the detection limit for TC detection is 97 nM. This method has been shown to be effective and reliable along with great promise for real-time visual monitoring of pH and TC values in real samples.

  • Bulletin of Materials Science | News

    • Dr Shanti Swarup Bhatnagar for Science and Technology

      Posted on October 12, 2020

      Prof. Subi Jacob George — Jawaharlal Nehru Centre for Advanced Scientific Research, Jakkur, Bengaluru
      Chemical Sciences 2020

      Prof. Surajit Dhara — School of Physics, University of Hyderabad, Hyderabad
      Physical Sciences 2020

    • Editorial Note on Continuous Article Publication

      Posted on July 25, 2019

      Click here for Editorial Note on CAP Mode

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