O M ZHIGALINA
Articles written in Bulletin of Materials Science
Volume 45 All articles Published: 17 February 2022 Article ID 0038
On the production of dispersive single-crystal iron carbide (Fe$_3$C) nanoparticulate
A N ZHIGACH I O LEIPUNSKY M L KUSKOV N G BEREZKINA E S AFANASENKOVA G W LOPEZ E A SKRYLEVA V P MENUSHENKOV O M ZHIGALINA D N KHMELENIN
In this study, the synthesis of uncontaminated, dispersible, single-crystal, stoichiometric iron carbide
(Fe$_3$C) nanoparticulate is pioneered successfully by using the flow-levitation (FL) method. The technique facilitates conditions forclean
and direct iron-carbon gas-phase reaction at high temperature, and for the purpose of this work, production regimes and parameters were
selected and customized in order to manufacture Fe$_3$C nanoparticles (NPs) of mean size 20 nm for subsequent characterization and evaluation.
Characterization is performed using analytical techniques that include transmission electron microscopy (TEM/HRTEM/STEM), electron and
X-ray diffraction, X-ray photoelectron spectroscopy, elemental CHNS analysis, specific surface area analysis and vibrating sample magnetometry
analysis. The results confirm the uncontaminated and stoichiometric character of the iron carbide NPs and demonstrate their
single-crystal nature. The synthesized product exhibits chemical inertness and excellent stability at room temperature over extended
periods of time. A detailed analysis of magnetic properties of the nanoparticulate was also performed. The saturation magnetization
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Volume 46, 2023
All articles
Continuous Article Publishing mode
Prof. Subi Jacob George — Jawaharlal Nehru Centre for Advanced Scientific Research, Jakkur, Bengaluru
Chemical Sciences 2020
Prof. Surajit Dhara — School of Physics, University of Hyderabad, Hyderabad
Physical Sciences 2020
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