• D K Walia

      Articles written in Bulletin of Materials Science

    • Study of Josephson effects in microbridges of Bi-Sr-Ca-Cu-O films made by spray pyrolysis

      D K Walia A K Gupta G S N Reddy V N Ojha V S Tomar Neeraj Khare N D Kataria K C Nagpal

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      Superconducting Bi-Sr-Ca-Cu-O (2212) films were prepared by spraying stoichiometric aqueous solutions of nitrates of bismuth, strontium, calcium and copper on heated MgO (100) substrates and subsequent annealing in air. TheR-T curves of the films show metallic behaviour above the superconducting transition temperature.Tc (R=0) is observed between 80 and 85 K. Annealing temperature has a profound effect onTc (R=0) and on the orientation of the film. Annealing in air in near-melting region yields highly oriented films withc-axis perpendicular to the substrate. These films show a sharp superconducting transition with zero resistance at 85 K. Microbridges of the dimensions of 50 µm × 50 µm have been patterned photolithographically followed with chemical etching. The 1 V characteristics of the microbridges show Josephson effects due to the presence of grain boundary weaklinks. The temperature dependence of the critical current for these microbridges suggest formation of superconductor-normal-superconductor type weaklinks.

    • Study of galvanomagnetic effects in Bi-Sr-Ca-Cu-O films

      Ramesh Chandra Neeraj Khare A K Gupta D K Walia Sangeeta Chaudhry V N Ojha V S Tomar

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      Galvanomagnetic effect has been studied at 77 K on Bi-Sr-Ca-Cu-O films as a function of d.c. bias current. These films were prepared by spray pyrolysis and screen-printing techniques, withTc (R=0) 80 K and 100 K respectively. Magnetic field dependence ofIc of sprayed-film showed very small hysteresis whereas screen-printed film showed greater hysteresis. Application of small magnetic field on these films destroyed the zero-resistance state and a finite resistance was developed. The slope of the resistance vs magnetic field curveΔR/ΔH depended on the current flowing through the sample. To increaseΔR/ΔH, meander-shape pattern was prepared on the sprayed film. In generalΔR/ΔH increased by a factor of 103 after sample patterning. The possibility of using these films as a sensitive magnetic field sensor is discussed.

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