• Amin Zadehnazari

      Articles written in Bulletin of Materials Science

    • Effect of amino acid-functionalized multi-walled carbon nanotubes on the properties of dopamine-based poly(amide–imide) composites: An experimental study

      Shadpour Mallakpour Amin Zadehnazari

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      In a single-step, rapid microwave-assisted process, multi-walled carbon nanotubes were functionalized by 𝑆-valine amino acid. Formation of amino acid on nanotube surface was confirmed by Fourier transform-infrared spectroscopy, thermogravimetric analysis, X-ray diffraction, field emission scanning and transmission electron microscopy techniques. The surface-modified nanotubes showed better chemical stability in common solvents such as 𝑁,𝑁-dimethylacetamide. The effects of amino acid functionalization of multiwalled carbon nanotubes on the properties of nanotube/poly(amide–imide) nanocomposites were investigated. The functionalized carbon nanotubes (5–15 wt%) were dispersed homogeneously in the poly(amide–imide) matrix, while the structure of the polymer and the nanotubes structure were stable in the preparation process as revealed by microscopic observations. The properties of nanocomposites were characterized extensively using the aforementioned techniques. The composite films have been prepared by casting a solution of precursor polymer containing 𝑆-valine-functionalized carbon nanotubes into a thin film and its tensile properties were examined. The Young’s modulus (elastic modulus) and tensile strength of the composite films were greatly improved by the incorporation of modified nanotubes.

    • Improved covalent functionalization of multi-walled carbon nanotubes using ascorbic acid for poly(amide–imide) composites having dopamine linkages


      More Details Abstract Fulltext PDF

      Ascorbic acid has been covalently linked to multi-walled carbon nanotubes (MWCNTs). The structures of the functionalized MWCNTs were characterized with Fourier-transform infrared spectroscopy. Thermogravimetric analysis results also demonstrated the presence of organic portions of the functionalized MWCNTs. Polymer composites based on a nanostructured poly(amide–imide) (PAI) were fabricated by an ex situ technique with 5, 10 and 15% loading by weight. Composite films were made by the solvent casting method. The thermal stabilityof the composites increased with even a small amount of modified MWCNT added. Tensile tests were conducted and depicted an increase in the elastic modulus with increasing MWCNTs content. X-ray diffraction study of thecomposites also indicated that the composites incorporated MWCNTs in the polymer chain.

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    • Dr Shanti Swarup Bhatnagar for Science and Technology

      Posted on October 12, 2020

      Prof. Subi Jacob George — Jawaharlal Nehru Centre for Advanced Scientific Research, Jakkur, Bengaluru
      Chemical Sciences 2020

      Prof. Surajit Dhara — School of Physics, University of Hyderabad, Hyderabad
      Physical Sciences 2020

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      Posted on July 25, 2019

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