• A K Ray

      Articles written in Bulletin of Materials Science

    • Fractography as well as fatigue and fracture of 25 wt% silicon carbide whisker reinforced alumina ceramic composite

      A K Ray S Banerjee E R Fuller S K Das G Das

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      Fatigue cracked and fast fractured regions in four-point bend specimens prepared from 25 wt% silicon carbide whisker reinforced alumina composite were examined by scanning electron microscopy. This composite was found to be susceptible to a fatigue crack growth phenomenon similar to that in the case of metallic materials, but with a higher crack growth exponent. In the fatigue region, the alumina matrix failed mainly in a transgranular mode and the whiskers mainly failed with a flat fracture surface but without their pullout. On the other hand, in the fast fracture region, the whiskers failed predominantly by pullout and the alumina matrix failed in a mixed mode with about half in transgranular and the other half in intergranular mode. Thus, to improve the fracture toughness of the material, the grain boundary strength of alumina and the matrix whisker interfacial bonding should be improved. To increase the resistance to fatigue, the fracture strength of the alumina grains should be improved by using finer α-alumina particles and the fatigue strength of the whisker have to be increased by improving the uniformity in distribution of β-SiC whiskers during hot pressing.

    • Studies on indentation fracture toughness on ceramic and ceramic composite using acoustic emission technique

      A K Ray G Das N K Mukhopadhyay D K Bhattacharya E S Dwarakadasa N Parida

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      This paper is aimed at investigating the acoustic emission activities during indentation toughness tests on an alumina based wear resistant ceramic and 25 wt% silicon carbide whisker (SiCw) reinforced alumina composite. It has been shown that the emitted acoustic emission signals characterize the crack growth during loading and unloading cycles in an indentation test. The acoustic emission results indicate that in the case of the composite the amount of crack growth during unloading is higher than that of loading, while the reverse is true in case of the wear resistant ceramics. Acoustic emission activity observed in wear resistant ceramic is less than that in the case of composite. An attempt has been made to correlate the acoustic emission signals with crack growth during indentation test.

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