A K Datta
Articles written in Bulletin of Materials Science
Volume 8 Issue 4 October 1986 pp 497-503
Structural changes accompanying thermal transformation in a chrysotile asbestos sample of Indian origin upto a temperature of 900°C have been investigated by x-ray method. The changes in lattice parameters have been systematically measured by applying a least square refinement technique and the crystallite size and strain defects at different stages have been estimated by line profile analysis of the diffraction peaks. The present study also confirms the earlier results on stepwise transformation of chrysotile fibres. This sequence of transformation has been explained assuming two different types of crystallites as reported in kaolinite.
Volume 9 Issue 2 June 1987 pp 103-110
Radial distribution analysis of x-ray intensities diffracted by chrysotile samples untreated and treated at different temperatures upto 900°C has been carried out. Interatomic distances, coordination numbers, mean square displacements and the interatomic coupling constants for different pairs of atoms have been calculated from the radial distribution curves. The interatomic distances and octahedral co-ordination number is found to decrease marginally upto 640°C and thereafter decrease steadily upto 800°C. The hydroxyl water is completely expelled from the structure and the original chrysotile structure breaks down. The entire process of dehydration has been interpreted in terms of RDF data.
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