• A K Nigam

      Articles written in Bulletin of Materials Science

    • One-pot size and shape controlled synthesis of DMSO capped iron oxide nanoparticles

      Debanjan Guin Sunkara V Manorama S Radha A K Nigam

      More Details Abstract Fulltext PDF

      We report here the capping of iron oxide nanoparticles with dimethyl sulfoxide (DMSO) to make chloroform soluble iron oxide nanoparticles. Size and shape of the capped iron oxide nanoparticles are well controlled by simply varying the reaction parameters. The synthesized nanocrystallites were characterized by thermal analysis (TG–DTA), powder X-ray diffraction (XRD), transmission electron microscopy (TEM) for evaluating phase, structure and morphology. 1H NMR spectra of the synthesized samples confirm DMSO, and the capping of DMSO on the ferrite samples. Shift of the S=O stretching frequency in Fourier transformed infrared (FTIR) spectra indicates that the bonding between DMSO and ferrite is through an oxygen moiety. The magnetic measurements of all the synthesized samples were investigated with a SQUID magnetometer which shows that the magnetic properties are strongly dependent on the size as well as shape of the iron oxide.

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