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    • In3+ doped magnesium ferrite an efficient magnetic catalyst for the synthesis of functionalized quinazolinone and Henry reaction

      NAIK M Z RODRIGUES , L TORNEY P S SALKER A V

      Volume 134 Published: 2 February 2022 Article ID 0019

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      https://www.ias.ac.in/article/fulltext/jcsc/134/0019

    • Keywords

       

      Henry reaction; quinazolinone; magnesium ferrite; In doped nanoparticles

    • Abstract

       

      Pristine and indium doped magnesium ferrite nanoparticles have been prepared by the sol-gelmethod. The phase formation has been confirmed from XRD (X-ray diffraction) whereas nanosize has beendisplayed through TEM (Transmission Electron Microscope) images. BET (Brunauer–Emmett–Teller)analysis showed an increase in surface area for the indium doped sample compared to pristine magnesiumferrite. The superparamagnetic nature of nanoparticles has been observed from M–H studies carried on VSMand these have been efficiently employed as a catalyst in organic transformation such as quinazolinonesynthesis and Henry reaction. The indium doped magnesium ferrite catalyst has been found to be highlyactive and recyclable in nature. The high surface area and Lewis acidity govern their catalytic performancewhereas magnetic nature makes the separation easier.

    • Graphical Abstract

       

    • Author Affiliations

       

      NAIK M Z1 RODRIGUES , L2 TORNEY P S2 SALKER A V2

      1. Carmel College of Arts, Science and Commerce for Women, Nuvem, India
      2. School of Chemical Sciences, Goa University, Panaji, India

    • Dates

       
      Published
      2 February 2022
      Manuscript received
      10 August 2021
      Manuscript revised
      23 September 2021
      Accepted
      12 October 2021

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