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Aryl azoxy compounds; arylazoxy sulfides; arylazo sulfides; aryldiazonium salts; aryl azo sulfones; arylazoxy sulfones; calvatic acid

An efficient, fast, and straightforward procedure for the synthesis of arylazoxy sulfides can be achieved by coupling reaction between aryl nitrasocompounds and tribenzenesulphenamide under microwave irradiation. Using the present method, different kinds of aryl nitrasocompounds containing various dioxolanerings and various tribenzenesulphenamide derivatives were rapidly converted to the corresponding arylazoxy sulfides in good yield and short reaction time. The use of non-toxic solvent, simple and clean work-up, short reaction times and good yields are the advantages of this method.

N MURTHY GANDIKOTA^{1 2} NARENDER MENDU² I V KASIVISWANATH³ R SEKHAR BOLLA¹ PRADEEP KUMAR BRAHMAN¹

1. Department of Chemistry, Koneuru Lakshmaiah Education Foundation, Vaddeswaram, Andhra Pradesh, India
2. GVK Biosciences, Hyderabad, Telangana 500076, India
3. Department of Basic Sciences and Humanities (Chemistry), Chalapathi Institute of Engineering and Technology (CIET), Lam, Guntur, Andhra Pradesh, India

Published

20 June 2020

Manuscript received

23 December 2019

Manuscript revised

12 February 2020

Accepted

23 February 2020