• Synthesis, characterization and crystal structure of new nickel molybdenum complex with the pyridine dicarboxylic acid ligand: Novel precursors for nickel molybdate nanoparticles

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      https://www.ias.ac.in/article/fulltext/jcsc/129/03/0373-0380

    • Keywords

       

      X-ray crystallography; NiMoO4; nanoparticles; electron microscopy.

    • Abstract

       

      A novel nickel molybdenum complex with the 2,6-pyridine dicarboxylic acid ligand was successfully synthesized and characterized by thermogravimetric analysis and single crystal X-ray crystallography. The single-crystal X-ray data revealed that the structure is a hydrated 1-D polymer with two different Ni sites.The synthesized complex was then used as a new precursor for the preparation of the related nickel molybdate nanoparticles. The crystallinity and morphology of the nickel molybdate nanoparticles were characterized by powder X-ray diffraction (XRD), energy-dispersive X-ray spectroscopy (EDS), scanning electron microscopy (SEM), transmittance electron microscopy (TEM), and Photoluminescence (PL) spectroscopy.

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  • Journal of Chemical Sciences | News

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