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Characteristic of silver nanowires prepared by polyol method based on orthogonal experimental design
HUI -MEI ZHANG YAN ZHANG JIA -WEN ZHANG XU YE YUAN -YUAN LI PING WANG
Volume 44 Published: 28 April 2021 Article ID 0117
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https://www.ias.ac.in/article/fulltext/boms/044/0117 -
Keywords
Silver nitrate ;AgNWs ;polyol method ;orthogonal experiment. -
Abstract
In this study, silver nanowires (AgNW$_s$) were prepared by the polyol method using silver nitrate (AgNO$_3$) asthe silver source and polyvinylpyrrolidone (PVP) as the structure-directing agent under different reaction conditions. Inorder to obtain AgNW$_s$ with good uniformity and electrical conductivity, the orthogonal experiment method was adopted to design an experimental scheme. The scanning electron microscope, energy-dispersive X-ray spectrometer, X-ray diffraction, UV-2550 UV–Visible spectrophotometer, transmission electron microscope, Fourier transform infrared and Raman spectra were combined to characterize synthesized AgNW$_s$. It can be concluded from experimental data that when the reaction temperature is 150$^{\circ}$C, the ratio of AgNO$_3$ to PVP is 1:3, the drop rate of PVP is 65 ml h$^{–1}$, with the existence of ferric chloride (FeCl3), and the AgNW$_s$ exhibit optimal morphology with the diameter ranging from 60 to 200 nm. The results in this study will provide experimental guide for controllable formation of AgNW$_s$.
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Author Affiliations
HUI -MEI ZHANG YAN ZHANG JIA -WEN ZHANG XU YE YUAN -YUAN LI PING WANG1
- National Engineering Laboratory for Modern Silk, College of Textile and Clothing Engineering, Soochow University, Suzhou 215000, China
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Dates
- Published
- 28 April 2021
- Manuscript received
- 13 July 2020
- Accepted
- 7 December 2020
- Final version published online
- 28 April 2021
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