• Gel combustion synthesis of fluorine-doped tin oxide and its characteristics: applying D-optimal factorial design of experiment

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      https://www.ias.ac.in/article/fulltext/boms/042/03/0109

    • Keywords

       

      Gel combustion; FTO; D-optimal factorial design; solar cells.

    • Abstract

       

      Fluorine-doped tin oxide (FTO) nano-powders were synthesized by a gel combustion method. To analyse the effect of processing factors and their interactions and to achieve an equation for nano-powder particle size in termsof code factors, D-optimal factorial design was used. Stannous chloride penta-hydride, ammonium fluoride and citric acid were used to synthesize the FTO nano-powders. The structure, morphology and composition of the synthesized powders were characterized by X-ray diffraction, field emission scanning electron microscopy and X-ray photoelectron spectroscopy, respectively. The results revealed the formation of homogenous FTO nano-powders with an average particle size of 20 nm and equiaxed morphology in the concentration of precursor 0.2, citric acid to precursor molar ratio of 1 and pH of 0.5. The average particle size increased as the concentration of the precursor, citric acid to precursor molar ratio and pH increased from 0.2 to 1, 1 to 3 and 0.5 to 3, respectively. Citric acid to precursor molar ratio, concentration of the precursor and the pH had the most significant effect on the synthesis of the FTO nano-powders, respectively.

    • Author Affiliations

       

      S MALEK1 S BAGHSHAHI2 R SARRAF-MAMOORY3 ALI NEMATI4

      1. Department of Materials Engineering, Science and Research Branch, Islamic Azad University, Tehran 1477893855, Iran
      2. Department of Materials Science and Engineering, Faculty of Engineering, Imam Khomeini International University, Qazvin 3414896816, Iran
      3. Department of Materials Engineering, Tarbiat Modares University, Tehran 1411713116, Iran
      4. Department of Materials Science and Engineering, Sharif University of Technology, Tehran 11365-9466, Iran
    • Dates

       
  • Bulletin of Materials Science | News

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