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      https://www.ias.ac.in/article/fulltext/boms/039/06/1501-1505

    • Keywords

       

      Co$_9$S$_8$ nanotubes; solvothermal; catalytic reduction; 4-nitrophenol.

    • Abstract

       

      Co$_9$S$_8$ nanotubes have been successfully synthesized via a facile two-step solvothermal method without the assistance of any template or surfactant, using cobalt sulphate (CoSO$_4$·7H$_2$O), urea and sodium sulphide (Na$_2$S·9H$_2$O) as starting reactants, and deionized water and glycol as the reactive medium. The phase and the morphologyof the as-obtained product were characterized by means of powder X-ray diffraction, energy dispersive spectrometry and scanning electron microscopy. The result displays that the Co9S8 nanotubes have hexagonal crosssections,the diameter of the nanotubes is about 200 nm and the wall thickness is of 50 nm. The experiments showed that the Co$_9$S$_8$ nanotubes could be used as new-type catalysts for the reduction of 4-nitrophenol. It was found thatthe as-obtained Co$_9$S$_8$ nanotubes contributed to the best catalytic activity.

    • Author Affiliations

       

      TAO GENG1 2 YONGHONG NI2 HONGYAN WANG1 XIA ZHOU1

      1. School of Chemistry and Chemical Engineering, Suzhou University, Suzhou 234000, PR China
      2. College of Chemistry and Materials Science, Key Laboratory of Functional Molecular Solids of Education Ministry, Anhui Laboratory of Molecule-Based Materials, Anhui Key Laboratory of Functional Molecular Solids, Annuli Normal University, Wuhu 241000, PR China
    • Dates

       
  • Bulletin of Materials Science | News

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