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      https://www.ias.ac.in/article/fulltext/boms/037/03/0425-0432

    • Keywords

       

      Spray pyrolysis techniques; TiO24 thin films; hydrogen gas response.

    • Abstract

       

      Nanostructured pure and Pt-doped TiO2 thin films were prepared by chemical spray pyrolysis technique. Aqueous solution of TiCl3.6H2O (0.01 M) was chosen as the starting solution for the preparation of pure TiO2 thin film. Aqueous solutions of PtCl6.6H2O (0.01 M) and TiCl3.6H2O (0.01 M) were mixed in volume % of 1 : 99, 2.5 : 97.5 and 5 : 95 respectively to obtain Pt-doped TiO2 thin films. The solutions were sprayed onto quartz substrate heated at 350 °C temperature to obtain the films. These thin films were fired for one hour at 550 °C. The sensing performance of these films was tested for various gases such as LPG, H2, CO2, ethanol, NH3 and Cl2 (1000 ppm). The Pt-doped TiO2 (1 : 99) was observed to be most sensitive (572) to H2 at 400 °C with high selectivity against other gases. Its response time was short (10 s) and recovery was also fast (14 s). To understand the reasons behind the gas-sensing performance of the films, their structural and micro-structral properties were studied using X-ray diffraction and electron microscopy (FE–SEM and TEM), respectively. Thicknesses of all these samples were determined using Surface Profiler. The results are interpreted.

    • Author Affiliations

       

      Lalchand A Patil1 Dinesh N Suryawanshi1 Idris G Pathan1 Dhanashri G Patil1

      1. Nanomaterials Research Lab, Department of Physics, Pratap College, Amalner 425 401, India
    • Dates

       
  • Bulletin of Materials Science | News

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      Prof. Surajit Dhara — School of Physics, University of Hyderabad, Hyderabad
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      Posted on July 25, 2019

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