• Fulltext

       

        Click here to view fulltext PDF


      Permanent link:
      https://www.ias.ac.in/article/fulltext/boms/034/06/1197-1199

    • Keywords

       

      Nanomaterials; calcium borate; synthesis.

    • Abstract

       

      Thorn-like polycrystalline Ca2B2O5.H2O microspheres with nano-sized slices were synthesized using boric acid and calcium hydroxide as reactants by a facile catalyst-free hydrothermal method at low temperature. The products were characterized by means of X-ray powder diffraction (XRD) and scanning electron microscopy (SEM). The XRD pattern reveals that the Ca2B2O5.H2O is a monoclinic phase polycrystalline with cell parameters 𝑎 = 0.6702, 𝑏 = 0.5419 and 𝑐 = 0.3558 nm. SEM also reveals that the monoclinic phase polycrystalline are thornlike microspheres composed of many flakes with an average thickness of <100 nm. Possible reaction and growth mechanism were also discussed.

    • Author Affiliations

       

      Guowei Zhao1 Laiping Zhang1 Jilin Wang1 Jie Li1 Qiongli Qian1 Xinye Pan1 Yunle Gu1 2

      1. School of Materials Science and Engineering, Wuhan Institute of Technology, Wuhan 430074, Hubei, China
      2. School of Materials Science and Engineering, Nano and Ceramic Materials Research Centre, Wuhan Institute of Technology, Wuhan 430074, Hubei, China
    • Dates

       
  • Bulletin of Materials Science | News

    • Editorial Note on Continuous Article Publication

      Posted on July 25, 2019

      Click here for Editorial Note on CAP Mode

© 2017-2019 Indian Academy of Sciences, Bengaluru.