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      https://www.ias.ac.in/article/fulltext/boms/034/04/0979-0983

    • Keywords

       

      MCM-41; mesoporous; super-microporous; hydrothermal stability.

    • Abstract

       

      Super-microporouos silicon material with high hydrothermal stability denoted as MCM-41-T has been prepared from mesoporous MCM-41 by high temperature treatment. The structural and chemical property of MCM-41-T has been characterized by X-ray diffraction, transmission electron microscopy, N2 adsorption-desorption, infrared spectroscopy and 29Si MAS NMR. The characteristic results show that Si–OH groups are forced to condense by high temperature treatment, and the pore size of MCM-41-T is around 1.5 nm in the super-microporous range. Compared with the original material MCM-41, the hydrothermal stability of MCM-41-T has been significantly enhanced.

    • Author Affiliations

       

      Shujie Wu1 Ke Song1 Jingqi Guan1 Qiubin Kan1

      1. College of Chemistry, Jilin University, Changchun 130023, P.R. China
    • Dates

       
  • Bulletin of Materials Science | News

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