• Fulltext

       

        Click here to view fulltext PDF


      Permanent link:
      https://www.ias.ac.in/article/fulltext/boms/032/02/0193-0197

    • Keywords

       

      Crystal growth; perovskites; PZT; hydrothermal method.

    • Abstract

       

      Pb(Zr0.52Ti0.48)O3 (PZT) powders were prepared by hydrothermal method. The effects of experimental parameters, including Pb/(Zr, Ti) ratio, alkaline concentration, reaction temperature and time on the product powders were studied in detail. Pure PZT powders were synthesized at suitable experimental conditions and Raman spectra confirmed the PZT with a perovskite-type structure. The homogeneous PZT powders with cubic-shaped morphology were formed at alkaline concentration of 1.2 M after reacting at 230°C for 2 h. The pure PZT powders obtained at low temperature and low alkaline concentration were attributed to precursors, TiCl4, with high activity and mineralizer NaOH with small cation radius.

    • Author Affiliations

       

      Zhong-Cheng Qiu1 Jian-Ping Zhou1 Gangqiang Zhu1 Peng Liu1 Xiao-Bing Bian1

      1. School of Physics and Information Technology, Shaanxi Normal University, Xi’an 710062, People’s Republic of China
    • Dates

       
  • Bulletin of Materials Science | News

    • Editorial Note on Continuous Article Publication

      Posted on July 25, 2019

      Click here for Editorial Note on CAP Mode

© 2017-2019 Indian Academy of Sciences, Bengaluru.