• Synthesis and structural studies of Na2O–ZnO–ZnF2–B2O3 oxyfluoride glasses

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      https://www.ias.ac.in/article/fulltext/boms/031/04/0631-0634

    • Keywords

       

      Borate glasses; oxyfluoride glasses; glass structure; MAS–NMR; IR.

    • Abstract

       

      This paper describes the synthesis and spectroscopic studies of the glass system, 20Na2O–(20–𝑥) ZnO–𝑥ZnF2–60B2O3 (𝑥 = 0, 5, 10, 15, 20), prepared by melt quenching method. The analyses of DSC and XRD did not show the crystallinity of the glass sample. 11B MAS–NMR shows the presence of sharp peak around –14 ppm. From the IR studies, the broadening of the peak around 1200–1400 and 800–1100 cm-1 shows the presence of mixed linkages like B–O–B, B–O–Zn in the network.

    • Author Affiliations

       

      Shantala D Patil1 V M Jali1 R V Anavekar2

      1. Department of Physics, Gulbarga University, Gulbarga 585 106, India
      2. Department of Physics, Bangalore University, Bangalore 560 056, India
    • Dates

       
  • Bulletin of Materials Science | News

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